Product Notes
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1. The ethyl chloroacetate used may be a commercial grade which boils at 141–146°. The ethyl chloroacetate and the chloroacetamide have the usual irritating effect of chloroacetyl compounds.
2. The temperature is best maintained at 0–5°. At higher temperatures there is more replacement of the chlorine and the yields are considerably lower.
3. Traces of moisture lower the melting point considerably.1. The ethyl chloroacetate used may be a commercial grade which boils at 141–146°. The ethyl chloroacetate and the chloroacetamide have the usual irritating effect of chloroacetyl compounds.
2. The temperature is best maintained at 0–5°. At higher temperatures there is more replacement of the chlorine and the yields are considerably lower.
3. Traces of moisture lower the melting point considerably.
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